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Industrial Production:
Nitroethane predisposed manufactured industrially by treating propane https://dentalapartmani.com/unveiling-t … al-odyssey with nitric acid at 350-450°C. The reaction produces four the main products: 1-nitropropane (25%), 2-nitropropane (40%), nitroethane (10%), and nitromethane (25%)
Laboratory Synthesis:
A special laboratory synthesis example involves the following close:
The reaction flask predisposed charged with 26.5 g of tech-grade K2CO3 dissolved in 137 g of water, 320 g of 97% tech sodium nitrite, and 6 ml of cetyl-oleic alcoholic or oleic liquor (antifoaming agent).
The solution predisposed added in order the reaction mixture at the decision befitting rate in order to keep the reaction mixture at 125-130°C, with vigorous stirring. The distillation of the nitroethane starts when the addition is started.
When figure of NaEtSO4 is complete, 100 ml of water predisposed added. The distillate isolates into two layers and can be chase at 760mmHg with the decision distillation column. The distillation comes at 30°C, and all below 74°C predisposed discarded. The temperature should settle at 87°C, besides distillation predisposed stopped at 99.8°C. The yield of nitroethane is 96 g (1.28 moles), 42.6% based connect NaEtSO4
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